4-ALLYLPHENOL
- Name 4-ALLYLPHENOL
- CAS 501-92-8
- Purity 99%
Product Details
Chinese Manufacturer Supply 4-ALLYLPHENOL 501-92-8 On Stock with Competitive Price
- Molecular Formula: C9H10O
- Molecular Weight: 134.178
- Vapor Pressure: 0.0282mmHg at 25°C
- Melting Point: 15.8°
- Refractive Index: 1.548
- Boiling Point: 238 °C at 760 mmHg
- PKA: 10.24±0.13(Predicted)
- Flash Point: 102.6 °C
- PSA： 20.23000
- Density: 1.014 g/cm3
- LogP: 2.12070
501-92-8 Relevant articles
Synthesis of 3-Methylobovatol
Pilkington, Lisa I.,Barker, David
, p. 2425 - 2428 (2015)
Biphenyl lignans are rare compounds that...
Magnolol derivative, honokiol derivative, hydrochloride of honokiol derivative, preparation method and application
-
Paragraph 0073-0074; 0084-0087, (2021/02/06)
The invention discloses a magnolol deriv...
Synthesis and Structural Revision of Glyphaeaside C
Byatt, Brendan J.,Kato, Atsushi,Pyne, Stephen G.
supporting information, p. 4029 - 4033 (2021/05/29)
The iminosugar core of natural glyphaeas...
Nickel-catalyzed reductive deoxygenation of diverse C-O bond-bearing functional groups
Cook, Adam,MacLean, Haydn,St. Onge, Piers,Newman, Stephen G.
, p. 13337 - 13347 (2021/11/20)
We report a catalytic method for the dir...
Structure–Activity Relationship of Anti-malarial Allylpyrocatechol Isolated from Piper betle
Horii, Toshihiro,Itagaki, Sawako,Kawano, Tomikazu,Miyoshi, Akihito,Murakami, Nobutoshi,Tamura, Satoru
, p. 784 - 790 (2020/09/18)
Malaria disease remains a serious worldw...
501-92-8 Process route
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-
140-67-0
Estragole
-
-
501-92-8
4-(prop-2-enyl)phenol
| Conditions | Yield |
|---|---|
|
With
aluminium(III) iodide; diisopropyl-carbodiimide;
In
acetonitrile;
at 80 ℃;
for 18h;
|
100%
|
|
With
boron tribromide;
In
dichloromethane;
at 0 ℃;
for 1h;
Inert atmosphere;
|
97.5%
|
|
With
dimethylsulfide; boron tribromide;
Heating;
|
95%
|
|
With
boron tribromide;
In
dichloromethane;
at 0 ℃;
for 1h;
|
95%
|
|
With
aluminium(III) iodide; diisopropyl-carbodiimide;
In
acetonitrile;
at 80 ℃;
for 18h;
|
91%
|
|
With
boron tribromide;
In
dichloromethane;
at -78 - 20 ℃;
|
89%
|
|
With
boron tribromide;
In
dichloromethane;
|
89%
|
|
With
boron trichloride-dimethyl sulfide;
In
trans-1,2-dichloroethylene; dichloromethane;
for 18h;
Reflux;
|
89%
|
|
With
aluminium(III) iodide;
In
dimethyl sulfoxide; acetonitrile;
at 80 ℃;
for 18h;
|
89%
|
|
With
aluminium(III) iodide; dimethyl sulfoxide;
In
acetonitrile;
at 80 ℃;
for 18h;
|
89%
|
|
With
boron tribromide;
In
dichloromethane;
for 0.833333h;
Ambient temperature;
|
85%
|
|
With
boron tribromide;
In
dichloromethane;
at 20 ℃;
for 1.33333h;
|
85%
|
|
With
boron tribromide;
In
dichloromethane;
at 20 ℃;
for 0.5h;
|
85%
|
|
With
boron tribromide;
In
dichloromethane;
at 0 ℃;
for 1h;
Inert atmosphere;
|
82%
|
|
Estragole;
With
aluminum (III) chloride; N,N-dimethyl-aniline;
In
toluene;
at 100 - 110 ℃;
for 2 - 3h;
With
hydrogenchloride; water;
In
toluene;
at 20 ℃;
pH=1 - 2;
Product distribution / selectivity;
|
81%
|
|
Estragole;
With
aluminum (III) chloride; N,N-dimethyl-1-naphthalenamine;
In
toluene;
at 100 - 110 ℃;
for 2 - 3h;
With
hydrogenchloride; water;
In
toluene;
at 20 ℃;
pH=1 - 2;
Product distribution / selectivity;
|
81%
|
|
With
methyl magnesium iodide;
at 180 ℃;
|
81%
|
|
With
boron tribromide;
In
dichloromethane;
at -10 - 0 ℃;
for 1h;
Inert atmosphere;
|
80.8%
|
|
Estragole;
With
boron tribromide;
In
dichloromethane;
at 0 - 20 ℃;
for 1.25h;
Inert atmosphere;
With
water;
In
dichloromethane;
Inert atmosphere;
|
73%
|
|
With
aluminium(III) iodide; calcium oxide;
In
acetonitrile;
at 80 ℃;
for 18h;
|
71%
|
|
With
boron tribromide;
In
dichloromethane;
at -78 - 15 ℃;
for 2h;
|
70%
|
|
With
boron tribromide;
In
dichloromethane;
at -78 - 20 ℃;
for 2h;
Inert atmosphere;
|
70%
|
|
With
boron tribromide;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
|
70.9%
|
|
With
methyl magnesium iodide;
|
64%
|
|
With
boron trichloride - methyl sulfide complex;
In
1,2-dichloro-ethane;
for 18h;
Reflux;
|
63%
|
|
With
boron tribromide;
In
dichloromethane;
at 0 ℃;
for 1h;
|
59%
|
|
With
boron tribromide;
In
dichloromethane;
at 0 - 20 ℃;
for 3h;
Inert atmosphere;
|
41%
|
|
Estragole;
With
aluminum (III) chloride; potassium iodide; diisopropyl-carbodiimide;
In
acetonitrile;
at 80 ℃;
for 18h;
With
hydrogenchloride;
In
water; acetonitrile;
|
38%
|
|
With
2,4,6-trimethyl-pyridine; lithium iodide;
for 22h;
Heating;
|
33%
|
|
With
boron tribromide;
In
dichloromethane;
at -78 - 20 ℃;
for 2h;
Inert atmosphere;
|
5.2%
|
|
With
ethyl bromide; magnesium; benzene;
Erhitzen des Reaktionsprodukts auf 150-160grad bei 10-15 mm Druck;
|
|
|
With
methyl magnesium iodide;
at 160 - 170 ℃;
for 3h;
|
|
|
With
boron tribromide;
In
dichloromethane;
|
25.27 g (56%)
|
|
Estragole;
With
water; boron trichloride; tetra-(n-butyl)ammonium iodide;
In
dichloromethane;
at -78 - 0 ℃;
for 2.11667h;
With
water;
for 0.5h;
|
|
|
Estragole;
With
boron tribromide;
In
chloroform;
at 23 - 26 ℃;
for 0.283333h;
With
sodium hydroxide; water;
at 20 ℃;
With
hydrogenchloride;
In
water;
at 20 ℃;
|
-
-
allylboronic acid N-methyl-iminodiacetic acid ester
-
-
106-48-9,82344-39-6
4-chloro-phenol
-
-
501-92-8
4-(prop-2-enyl)phenol
| Conditions | Yield |
|---|---|
|
With
potassium carbonate;
In
water;
at 135 ℃;
for 0.3h;
Microwave irradiation;
Sealed tube;
|
75%
|
501-92-8 Upstream products
-
140-67-0
Estragole
-
917-64-6
methyl magnesium iodide
-
94-59-7
1-allyl-3,4-methylenedioxybenzene
-
32704-23-7
4-(2-propenyl)aniline
501-92-8 Downstream products
-
528-43-8
Magnolol
-
59877-61-1
HO-NBA
-
140-67-0
Estragole
-
108886-90-4
1-allyl-4-oxocyclohexa-2,5-dienylethanoate
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